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Process Flow of Biodiesel Separation Using a Disc Stack Centrifuge
Disc stack centrifuges are widely used in biodiesel production to efficiently separate glycerol, catalyst residues, unreacted oils, and other impurities from the crude biodiesel mixture after the transesterification reaction. Below is a detailed workflow and key considerations:
Pre-Treatment:
Reaction Mixture Preparation: After transesterification (oil + methanol + catalyst), the mixture contains biodiesel, glycerol, methanol, and catalyst residues.
Settling (Optional): Allow the mixture to settle briefly in a tank to separate a portion of glycerol (heavier phase) via gravity.
Centrifugal Separation:
Feeding: Pump the crude biodiesel mixture into the disc stack centrifuge.
Separation Parameters:
Speed: 6,000-10,000 rpm (adjust based on viscosity and impurity content).
Temperature: Maintain at 50-70°C to reduce viscosity and improve separation efficiency.
Phase Separation:
Heavy Phase (Glycerol + Catalyst): Deposited along the centrifuge bowl wall and discharged through the heavy-phase outlet.
Light Phase (Biodiesel + Methanol): Collected via the light-phase outlet.
Continuous Operation: Industrial systems enable uninterrupted processing for large-scale production.
Post-Treatment:
Methanol Recovery: Distill methanol from the light phase for reuse.
Biodiesel Washing: Wash the biodiesel with water to remove residual catalyst and soap.
Final Drying: Remove water traces using vacuum dryers or adsorption filters.
Glycerol Purification: Refine the glycerol phase for commercial use (e.g., cosmetics, pharmaceuticals).
High Efficiency: Rapid separation of immiscible phases (biodiesel/glycerol) with minimal downtime.
Scalability: Suitable for batch or continuous processing (1-100+ tons/hour).
Purity: Achieves biodiesel purity >98%, meeting ASTM D6751/EN 14214 standards.
Automation: Integrated PLC systems enable precise control of flow rates and separation parameters.
Feed Quality: Ensure consistent feedstock composition (e.g., FFA content <0.5%) to avoid emulsification.
Temperature Control: Overheating may degrade biodiesel; monitor closely.
Maintenance: Regularly clean disc stacks to prevent fouling by soap or solids.
Waste Handling: Treat glycerol phase and wash water per environmental regulations.
Industrial Biodiesel Plants: Primary separation of biodiesel from glycerol.
Feedstock Flexibility: Compatible with vegetable oils (e.g., soybean, rapeseed) and waste cooking oils.
Byproduct Recovery: High-purity glycerol for pharmaceutical or chemical industries.
Gravity Settling Tanks: Low cost but slow (24-48 hours) and less efficient.
Membrane Filtration: Effective for fine impurities but prone to clogging and high energy use.
Three-Phase Centrifuges: Separate biodiesel, glycerol, and solids simultaneously but require complex operation.
By integrating disc stack centrifuges into biodiesel production, manufacturers achieve higher yields, reduced processing time, and compliance with global biodiesel quality standards.
During the dep processing in the breeding industry, the use of separators can help oil recovery in the processing of subsidiary materials, which not only enhances profits, but also reduces pollution emission.
Three separation disc type separator centrifuge for animal oil factory is mainly used in refining meat oil from animals such as fishmeal facotry,animal oil factory, the capacity from 10t/d~600t/d.
This special design separator has the full automatic control box which used for safety protection and equips and also been equipped with advanced automatic vibration tester which can view vibrating value at any time. We can make separating and discharging to the best affection from regulating separation parameter directly at the screen.
It has advantages of high speed, smooth operating, compact structure, small footprint, all sealed of the inlet and discharge, low noise, good separation. The materials of centrifuge which contact with the parts are stainless steel which meets the requirements of food grade.
Main parameter
|
DPF 445
|
DPF 530
|
DPF 550
|
Bowl Inner Diameter
|
445 mm
|
530 mm
|
550 mm
|
Disc Number
|
73
|
80
|
110
|
Bowl Rotating Speed
|
5100 rpm
|
4650 rpm
|
4500 rpm
|
Separating Factor
|
6480
|
6400
|
6230
|
Capacity
|
35000~40000 L/h
|
45000 L/h
|
75000 L/h
|
Motor Power
|
37 Kw
|
37 Kw
|
55 Kw
|
Nozzle
|
10
|
10
|
12
|
Dimension (L×W×H) mm
|
1503×1129×1516
|
1430×1174×1544
|
2044×1320×1954
|
Weight (kg)
|
1100
|
1550
|
2100
|
Warranty
|
1 year
|
1 year
|
1 year
|
Product model list
Model | Flowrate | Inlet pressure | Outlet pressure | Power | Weight |
DHZ470 | 2500-7000 LPH | 0.05 MPA | 0.1-0.25 MPA | 15 KW | 1880 KG |
Product Advantage
1. Continuous feeding
2. High separation factor
3. Automatic residue discharging
4. Concise bowl design without frequent washing
5. Hydraulic coupling driving with longer service
6. PLC system automatic control